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Microstructure and corrosion performance of 316L stainless steel fabricated by Selective Laser Melting and processed through high-pressure torsion

Mohd Yusuf, S; Nie, M; Chen, Y; Yang, S; Gao, N; (2018) Microstructure and corrosion performance of 316L stainless steel fabricated by Selective Laser Melting and processed through high-pressure torsion. Journal of Alloys and Compounds , 763 pp. 360-375. 10.1016/j.jallcom.2018.05.284. Green open access

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Abstract

For the first time, the novel combination of severe plastic deformation (SPD) and Additive Manufacturing (AM) in a single process sequence was explored. 316L stainless steel (316L SS) alloy was firstly fabricated by Selective Laser Melting (SLM) AM process and subsequently processed by high-pressure torsion (HPT) SPD technique under a constant pressure of 6 GPa for different torsional revolutions. All the processed samples were subjected to electrochemical testing in a 3.5 wt % NaCl aqueous solution using open-circuit potential, potentiodynamic polarisation, and electrochemical impedance spectroscopy techniques, and characterised with scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The microscopic measurement results revealed that the melt pools and cellular structures obtained via SLM become increasingly refined through increased HPT revolutions, accompanied by significant porosity reduction and significant increase in microhardness. TEM observations revealed a homogeneously distributed nano-scale grains after 10 turns. Moreover, the results demonstrated that HPT processing significantly enhances corrosion performance of the 316L SS alloy in NaCl solution, due to the cellular structure refinement, homogeneous microstructure distribution, and the substantial removal of pores and defects. SEM and energy dispersive x-ray spectroscopy (EDX) analysis were also carried out on the corroded samples to determine the influence of cellular structure refinement on the corrosion characteristics of the 316L SS alloy.

Type: Article
Title: Microstructure and corrosion performance of 316L stainless steel fabricated by Selective Laser Melting and processed through high-pressure torsion
Open access status: An open access version is available from UCL Discovery
DOI: 10.1016/j.jallcom.2018.05.284
Publisher version: https://doi.org/10.1016/j.jallcom.2018.05.284
Language: English
Additional information: This version is the author accepted manuscript. For information on re-use, please refer to the publisher’s terms and conditions.
Keywords: Selective Laser Melting, High-pressure Torsion, 316L stainless steel, Microhardness, Corrosion behaviour
UCL classification: UCL
UCL > Provost and Vice Provost Offices > UCL BEAMS
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Maths and Physical Sciences
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Maths and Physical Sciences > MAPS Faculty Office
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Maths and Physical Sciences > MAPS Faculty Office > Institute for Materials Discovery
URI: https://discovery-pp.ucl.ac.uk/id/eprint/10049390
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