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High-resolution 3D strain and orientation mapping within a grain of a directed energy deposition laser additively manufactured superalloy

Chen, Y; Tang, YT; Collins, DM; Clark, SJ; Ludwig, W; Rodriguez-Lamas, R; Detlefs, C; ... Yildirim, C; + view all (2023) High-resolution 3D strain and orientation mapping within a grain of a directed energy deposition laser additively manufactured superalloy. Scripta Materialia , 234 , Article 115579. 10.1016/j.scriptamat.2023.115579. Green open access

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Abstract

The industrialization of Laser Additive Manufacturing (LAM) is challenged by the undesirable microstructures and high residual stresses originating from the fast and complex solidification process. Non-destructive assessment of the mechanical performance controlling deformation patterning is therefore critical. Here, we use Dark Field X-ray Microscopy (DFXM) to map the 3D subsurface intragranular orientation and strain variations throughout a surface-breaking grain within a directed energy deposition nickel superalloy. DFXM results reveal a highly heterogenous 3D microstructure in terms of the local orientation and lattice strain. The grain comprises ≈ 5 μm-sized cells with alternating strain states, as high as 5 x 10^{-3}, and orientation differences <0.5°. The DFXM results are compared to Electron Backscatter Diffraction measurements of the same grain from its cut-off surface. We discuss the microstructure developments during LAM, rationalising the development of the deformation patterning from the extreme thermal gradients during processing and the susceptibility for solute segregation.

Type: Article
Title: High-resolution 3D strain and orientation mapping within a grain of a directed energy deposition laser additively manufactured superalloy
Open access status: An open access version is available from UCL Discovery
DOI: 10.1016/j.scriptamat.2023.115579
Publisher version: https://doi.org/10.1016/j.scriptamat.2023.115579
Language: English
Additional information: This version is the author accepted manuscript. For information on re-use, please refer to the publisher's terms and conditions.
Keywords: Directed energy deposition, Laser additive manufacturing, Dark field x-ray microscopy, Electron backscatter diffraction, Microstructure
UCL classification: UCL
UCL > Provost and Vice Provost Offices > UCL BEAMS
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Engineering Science
UCL > Provost and Vice Provost Offices > UCL BEAMS > Faculty of Engineering Science > Dept of Mechanical Engineering
URI: https://discovery-pp.ucl.ac.uk/id/eprint/10171766
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